HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 499625Generated: October 31, 2026
HCID 59750101, compound → HCID 59750357, compound
https://huagongshe.com/reaction/499625
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 59750101 | HCID 59750101 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 59750357 | HCID 59750357 | 82.2% |
Reaction Steps
tert-Butyl [2-oxo-3-[2-(4-oxo-4H-1,3-benzothiazin-2-yl)-4-pyridyl]-1-imidazolidinyl]acetate (0.31 g, 0.70 mmol) was dissolved in trifluoroacetic acid (5 ml), and the mixture was stirred at 0° C. for 2 hrs. The solvent was evaporated and the residue was recrystallized from diethyl ether-methanol to give the titled compound (0.22 g, 81%) as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07767665B2 |
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| Source dataset | uspto-grants-2010_08 |
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| ORD ID | ord-710dfad0d4c94dfc89f1ff7a0013603d |
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| Source note | uspto-grants-2010_08 |
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