1-Bromononane → 4-[Hydroxy(diphenyl)methyl]-1-nonyl-1-azoniabicyclo[2.2.1]heptane bromide

Participants

Reaction Steps

Following the general procedure outlined in Example 2, 1-azabicyclo[2.2.1]hept-4-yl(diphenyl)methanol (29.3 mg, 0.105 mmol) and 1-bromononane (0.04 mL, 0.2 mmol) in 2 CH3CN/3 CHCl3 (2.5 mL) were reacted to give the desired product (31.5 mg, 62%). EI-MS m/z 407 (M+) Rt (2.23 min).

Provenance & Evidence