HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, (2-bromoethoxy)- → HCID 16041580, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, (2-bromoethoxy)- | HCID 68526 | — |
| Reactant | 1-Azabicyclo[2.2.1]hept-4-yl(diphenyl)methanol | HCID 42625856 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 16041580 | HCID 16041580 | 62.6% |
Reaction Steps
Following the general procedure outlined in Example 2, 1-azabicyclo[2.2.1]hept-4-yl(diphenyl)methanol (30.8 mg, 0.110 mmol) and 2-bromoethyl phenyl ether (35.7 mg, 0.177 mmol) in 2 CH3CN/3CHCl3 (2.5 mL) were reacted to give the desired product (33.1 mg, 62%). EI-MS m/z 400 (M+) Rt (1.86 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767691B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-4d5d89f3fbde4c9ca323dda131f791c1 |
| Source note | uspto-grants-2010_08 |