HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 24694511, compound → HCID 16041588, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 24694511 | HCID 24694511 | — |
| Reactant | 1-Azabicyclo[2.2.1]hept-4-yl(diphenyl)methanol | HCID 42625856 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 16041588 | HCID 16041588 | 37% |
Reaction Steps
Following the general procedure outlined in Example 2, 1-azabicyclo[2.2.1]hept-4-yl(diphenyl)methanol (33.0 mg, 0.118 mmol) and 1-{[(2-bromoethyl)oxy]methyl}-3-(methyloxy)benzene (42.5 mg, 0.173 mmol) in 2 CH3CN/3 CHCl3 (2.5 mL) were reacted to give the desired product (22.8 mg, 37%). EI-MS m/z 444 (M+) Rt (1.96 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767691B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-874981e383dc417ca7bc0026d6b91e36 |
| Source note | uspto-grants-2010_08 |