HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-1-hexanol → HCID 16041762, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-1-hexanol | HCID 77970 | — |
| Reactant | 1-Azabicyclo[2.2.1]hept-4-yl(diphenyl)methanol | HCID 42625856 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 16041762 | HCID 16041762 | 6% |
Reaction Steps
Following the general procedure outlined in Example 1, 1-azabicyclo[2.2.1]hept-4-yl(diphenyl)methanol (32.0 mg, 0.116 mmol) and 6-bromo-1-hexanol (0.03 mL, 0.248 mmol) in 2 CH3CN/3 CHCl3 (2.5 mL) were reacted to give the desired product (3 mg, 6%). EI-MS m/z 380 (M+) Rt (1.64 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767691B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-7c0b6660fa8e4130aa238be6723a918b |
| Source note | uspto-grants-2010_08 |