HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromohexane → HCID 16042139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromohexane | HCID 8101 | — |
| Reactant | HCID 42625857 | HCID 42625857 | — |
| Product | HCID 16042139 | HCID 16042139 | 44.4% |
Reaction Steps
Following the general procedure outlined in Example 24, 1-azabicyclo[2.2.1]hept-4-yl(diphenyl)acetonitrile (0.044 g, 0.152 mmol) and 1-bromohexane (0.035 mL, 0.249 mmol) in 2CH3CN/3CHCl3 (3.5 mL) were reacted to give the desired product (0.0306 g, 44.3%). EI-MS m/z 373 (M+) Rt (1.83 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767691B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-f1baf6f3f7b3453abbcdd6a7b5223581 |
| Source note | uspto-grants-2010_08 |