HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Bromoethyl)-1H-indole → HCID 16042145, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Bromoethyl)-1H-indole | HCID 22262670 | — |
| Reactant | HCID 42625857 | HCID 42625857 | — |
| Product | HCID 16042145 | HCID 16042145 | 43.6% |
Reaction Steps
Following the general procedure outlined in Example 24, 1-azabicyclo[2.2.1]hept-4-yl(diphenyl)acetonitrile (0.044 g, 0.152 mmol) and 2-(2-bromoethyl)-1H-indole (0.0494 g, 0.220 mmol) in 2CH3CN/3CHCl3 (3.5 mL) were reacted to give the desired product (0.0340 g, 43.4%). EI-MS m/z 432 (M+) Rt (1.94 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767691B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-bda9cd49c64048a1a8605f44e109bc05 |
| Source note | uspto-grants-2010_08 |