HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromobutyronitrile → HCID 68460432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromobutyronitrile | HCID 21412 | — |
| Reactant | HCID 42625857 | HCID 42625857 | — |
| Product | HCID 68460432 | HCID 68460432 | 54.3% |
Reaction Steps
Following the general procedure outlined in Example 24, 1-azabicyclo[2.2.1]hept-4-yl(diphenyl)acetonitrile (0.044 g, 0.152 mmol) and 4-bromobutanenitrile (0.025 mL, 0.252 mmol) in 2CH3CN/3CHCl3 (3.5 mL) were reacted to give the desired product (0.0360 g, 54.1%). EI-MS m/z 356 (M+) Rt (1.57 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767691B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-0b522347f5374d24ad9be9f4c99f2d6e |
| Source note | uspto-grants-2010_08 |