HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrophenyl chloroformate → HCID 11842627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| Reactant | 4-(4-Aminophenoxy)-N-methylpicolinamide | HCID 16655129 | — |
| Reactant | HCID 16769139 | HCID 16769139 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 11842627 | HCID 11842627 | — |
Reaction Steps
2.2 Analogously to Example 1.3, reaction of “2a” with 4-nitrophenyl chloroformate and N-methyl-4-(4-aminophenoxy)pyridine-2-carboxamide gives the compound “2”; TLC in dichloromethane/methanol 9/1 Rf=0.63; HPLC-APCI-MS [M+H+] 509
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767696B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-7cc88d1d9e7d4164aea8436f68d87df5 |
| Source note | uspto-grants-2010_08 |