2,4,6-Tris(benzyloxy)benzoic acid → HCID 57480142, compound

HRID 499756Notes

Reaction equation

HRID 499756 reaction equation
[CH2:1]([O:8][C:9]1[CH:17]=[C:16]([O:18][CH2:19][C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH:15]=[C:14]([O:26][CH2:27][C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[C:10]=1[C:11](O)=[O:12])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[OH:34][C:35]1[CH:36]=[C:37]([CH2:41][C:42]([NH:44][NH2:45])=[O:43])[CH:38]=[CH:39][CH:40]=1>>[OH:34][C:35]1[CH:36]=[C:37]([CH2:41][C:42]([NH:44][NH:45][C:11](=[O:12])[C:10]2[C:14]([O:26][CH2:27][C:28]3[CH:29]=[CH:30][CH:31]=[CH:32][CH:33]=3)=[CH:15][C:16]([O:18][CH2:19][C:20]3[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=3)=[CH:17][C:9]=2[O:8][CH2:1][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)=[O:43])[CH:38]=[CH:39][CH:40]=1

Participants

3

Reactant 2

HCID 574612342,4,6-Tris(benzyloxy)benzoic acidHCID 5975460620277-01-4

Product 1

HCID 57480142HCID 57480142, compoundYield 40%

Procedure

The coupling of 2,4,6-tribenzyloxybenzoic acid to (3-hydroxyphenyl)acetohydrazide is carried out analogously to Example 2.5, giving N′-[2-(3-hydroxyphenyl)acetyl]-2,4,6-tribenzyloxybenzohydrazide, yield 40%; m.p. 154-155°.

Sources & evidence

ORD record
ord-eb621c0ecb0e4f10823391cccf9d6851
Source dataset
uspto-grants-2010_08
Patent number
US07767716B2

Reaction notes

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