Ethylamine → 3,5-Dichloro-N-ethyl-2-hydroxybenzamide

HRID 499855Notes

Reaction equation

HRID 499855 reaction equation

[Cl:1][C:2]1[C:3]([OH:12])=[C:4]([CH:8]=[C:9]([Cl:11])[CH:10]=1)[C:5]([OH:7])=O.[CH2:13]([NH2:15])[CH3:14]>>[Cl:1][C:2]1[C:3]([OH:12])=[C:4]([CH:8]=[C:9]([Cl:11])[CH:10]=1)[C:5]([NH:15][CH2:13][CH3:14])=[O:7]

Participants

3

Reactant 2

HCID 6341Ethylamine

HCID 94453,5-Dichlorosalicylic acid

Product 1

HCID 539124643,5-Dichloro-N-ethyl-2-hydroxybenzamide

Procedure

Prepared from 3,5-dichloro-2-hydroxybenzoic acid and ethylamine using the method of preparation 57 to give the title compound as a pale yellow solid.

Workup

customthe method of preparation 57

Sources & evidence

ORD record: ord-898b6f119a3a462abd4f560b6122cdcf
Source dataset: uspto-grants-2010_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07767715B2

Reaction notes

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