참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 1-Chloro-3-(diethylamino)-2-propanol | HCID 5298859 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N,N-Diethyl-2-oxiranemethanamine | HCID 95611 | 76% |
반응 단계
A solution of sodium hydroxide (47.9 g, 1.2 mole) in 78 mL water was added 1-chloro-3-diethylamino-propan-2-ol. The resultant was stirred at 20-25° C. for 1 hour, diluted with 178 mL of water and extracted with ether twice. The combined ether solution was dried with solid potassium hydroxide and evaporated to give 135 g of crude product which was purified by fraction distillation to give pure glycidyldiethylamine (98 g, 76%) as an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06710067B2 |
|---|
| 출처 데이터셋 | uspto-grants-2004_03 |
|---|
| ORD ID | ord-09011d018c3949968bf68fa8fbed931f |
|---|
| 출처 메모 | uspto-grants-2004_03 |
|---|
