HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67225149, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | tert-Butyl {2-[(pyridin-2-yl)oxy]ethyl}carbamate | HCID 68804906 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67225149 | HCID 67225149 | 96.8% |
Reaction Steps
tert-Butyl 2-(pyridin-2-yloxy)ethylcarbamate (0.353 g) was treated with 4M of hydrogen chloride in 1,4-dioxane (0.6 mL) at RT for 1 h. The solvent was evaporated under reduced pressure. The residue was washed with ether, and dried to give the desired product (0.30 g, 96.8%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767675B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-c5742f2cdaee4c8e8d46c7cd0e7629ae |
| Source note | uspto-grants-2010_08 |