HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethylisoxazole-4-isocyanate → 1-(3,5-Dimethylisoxazol-4-yl)carbamoylcyclopropanesulfonamide tert-butylcarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethylisoxazole-4-isocyanate | HCID 2736266 | — |
| Reactant | 1-Methoxymethylcyclopropylsulfonylamine tert-butylcarbamate | HCID 66752382 | — |
| Product | 1-(3,5-Dimethylisoxazol-4-yl)carbamoylcyclopropanesulfonamide tert-butylcarbamate | HCID 66752480 | 100% |
Reaction Steps
This compound was obtained in a crude 100% yield according to the procedure described for the synthesis of 1-methoxymethylcyclopropylsulfonylamine tert-butylcarbamate except that 1.20 equivalents of 3,5-dimethylisoxazole-4-isocyanate was used as the electrophile. The compound was taken directly into the next reaction without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07772180B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-ff598d96d2ea4b16b39088dd92608f84 |
| Source note | uspto-grants-2010_08 |