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HRID50057

反应详情

EQUATION

反应方程式

HRID 50057 的结构方程式

REACTANTS

反应物

1
结构：COC(=O)CCC(C#N)(CCC(=O)[O-])c1ccc(Cl)c(Cl)c1
HCID22741721

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)CCC1(c2ccc(Cl)c(Cl)c2)CCC(=O)NC1
HCID22741813

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Ni]
催化剂HCID935

Nickel

Ni

结构：COCCO
溶剂HCID8019

2-Methoxyethanol

C3H8O2

PROCEDURE

实验过程

40 g of the compound prepared in step A are dissolved in 500 ml of 2-methoxyethanol, 2 g of Raney nickel are added and the mixture is hydrogenated at 40° C. under atmospheric pressure for 3 days. It is filtered and evaporated to give the expected product in the form of an oil (39 g).

WORKUP

后处理

  1. filtrationIt is filtered
  2. customevaporated