Benzoyl Peroxide → HCID 21931910, compound

Participants

Reaction Steps

A mixture of 7-chloro-1-methyl-dibenzofuran (6.27 g, 29.1 mmol), N-bromosuccinimide (5.4 g, 30.3 mmole) and dibenzoyl peroxide (0.82 g, 3.4 mmole) in tetrachlorocarbon (100 mL) was heated at reflux for 3 hours, and then concentrated to about 50 mL. The resulting suspension was filtered, rinsed by CCl4. The solid was dissolved in CH2Cl2, washed by water, dried over Na2SO4, evaporated to give 6.16 g of beige solid.

Provenance & Evidence