HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxy-4-nitrophenol → HCID 59424650, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxy-4-nitrophenol | HCID 12900532 | — |
| Reactant | 7-chloro-2-(1-methyl-1H-imidazol-2-yl)-thieno[3,2-b]pyridine | HCID 22143563 | — |
| Reactant | 7-(2-Fluoro-4-nitrophenoxy)-2-(thiazol-2-yl)thieno[3,2-b]pyridine | HCID 59424425 | — |
| Product | HCID 59424650 | HCID 59424650 | 9% |
Reaction Steps
Starting from compound 214, following the procedure described above for the synthesis of compound 11 (scheme 2, step 3, example 12) but replacing 2-fluoro-4-nitrophenol with 3-methoxy-4-nitrophenol [Hodgson, C., J. Chem. Soc., 1929, 2778], title compound 215 was obtained in 9% yield. MS (m/z) 383.1 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07772247B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-d36675e76d454012aa56d627a95876d0 |
| Source note | uspto-grants-2010_08 |