HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-1-methyl-1H-imidazole → HCID 59424524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-1-methyl-1H-imidazole | HCID 1277653 | — |
| Reactant | 7-Chloro-2-(1,3-thiazol-2-yl)thieno[3,2-b]pyridine | HCID 22143663 | — |
| Reactant | 7-Chloro-2-(tributylstannyl)thieno[3,2-b]pyridine | HCID 57516658 | — |
| Product | HCID 59424524 | HCID 59424524 | 29% |
Reaction Steps
Starting from the compound 98 (scheme 19), following the procedure described above for the synthesis of compound 10 (scheme 2, step 2, example 12) but replacing 2-bromothiazole with 4-bromo-1-methyl-1H-imidazole, title compound 224 was obtained in 29% yield. MS (m/z): 250.1 (100%), 252.1 (37%) (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07772247B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-fbe0f98350d946788be551c222aaad25 |
| Source note | uspto-grants-2010_08 |