HRID501417

反应详情

EQUATION

反应方程式

HRID 501417 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture consisting of 10 g of benzyl 3-t-butoxycarbonylaminopiperidine-1-carboxylate, 500 mg of 10% palladium carbon and 100 ml of ethanol was stirred at room temperature under a hydrogen atmosphere overnight. The catalyst was removed by filtration. The filtrate was concentrated and dried to give 6.0 g of the title compound.

WORKUP

后处理

  1. customThe catalyst was removed by filtration
  2. concentrationThe filtrate was concentrated
  3. customdried