HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 501490Generated: October 29, 2026
Ethylmorpholine → HCID 72412476, compound
https://huagongshe.com/reaction/501490
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethylmorpholine | HCID 7525 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | N-Hydroxy-1,1,1-trimethylsilanamine | HCID 21936899 | — |
| Reactant | HCID 68459175 | HCID 68459175 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 72412476 | HCID 72412476 | — |
Reaction Steps
200 mg (0.55 mmol) of 1-(4-methanesulfonylbenzenesulfonyl)octahydrocyclopenta-[b]pyrrole-2-carboxylic acid were dissolved in 10 ml of DMF, after which 0.60 mmol of ethyl chloroformate, 1.22 mmol of N-ethylmorpholine and 1.67 mmol of trimethylsilylhydroxylamine were added. After the mixture had been heated at 80° C. for 4 h, the solvent was removed under reduced pressure and the crude product was purified using chromatographic methods.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07772270B2 |
|---|
| Source dataset | uspto-grants-2010_08 |
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| ORD ID | ord-9fa46e8e34e542699721ebd9e27b19d7 |
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| Source note | uspto-grants-2010_08 |
|---|
