Phenyl isocyanate → HCID 68461014, compound

Participants

Reaction Conditions

Reaction Steps

500 mg (1.30 mmol) of 1-(4′-aminobiphenyl-4-sulfonyl)octahydrocyclopenta[b]pyrrole-2-carboxylic acid were dissolved in 3 ml of DMF, after which the solution was cooled down to 0° C. in an ice bath and 1.4 mmol of phenylisocyanate were added. The reaction solution was then stirred at RT for a further 4 h. The crude product was purified using chromatographic methods.

Provenance & Evidence