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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 501504Generated: October 26, 2026

Azobisisobutyronitrile → Prop-2-enenitrile--ethenylbenzene (1/1)

https://huagongshe.com/reaction/501504

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAzobisisobutyronitrileHCID 6547—
ReactantStyreneHCID 7501—
ReactantAcrylonitrileHCID 7855—
ReactantTricalcium PhosphateHCID 24456—
SolventWaterHCID 962—
ProductProp-2-enenitrile--ethenylbenzene (1/1)HCID 62696—

Reaction Steps

72 parts of styrene, 28 parts of acrylonitrile, and 120 parts of deionized water are mixed. To the mixture, 0.2 parts of azobisisobutylonitrile (AIBN), 0.4 parts of tricalcium phosphate and 0.2 parts of mercaptan-containing chain transfer agent are added. The resultant solution is heated to 80° C. for 90 minutes and kept for 180 minutes. The resultant is washed, dehydrated and dried to obtain styrene-acrylonitrile copolymer resin (SAN) in powder form.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07772303B2
Source datasetuspto-grants-2010_08
ORD IDord-89cfc22dadac4e29aac79744d92ae7de
Source noteuspto-grants-2010_08