4-Isocyanato-5,6,7,8-tetrahydronaphthalene-1-carbonitrile → 2-Chloro-4-isocyanato-3-methylbenzonitrile

HRID 501564Notes

Reaction equation

HRID 501564 reaction equation
[Cl:1][C:2]1[C:3]([CH3:17])=[C:4]([NH:10][C:11]2C=CC=CC=2)[CH:5]=[CH:6][C:7]=1[C:8]#[N:9].Cl.NC1C2CCCCC=2C(C#N)=CC=1.N(C1C2CCCCC=2C(C#N)=CC=1)=C=[O:34]>>[Cl:1][C:2]1[C:3]([CH3:17])=[C:4]([N:10]=[C:11]=[O:34])[CH:5]=[CH:6][C:7]=1[C:8]#[N:9]

Participants

4

Reactant 3

HCID 597543044-Isocyanato-5,6,7,8-tetrahydronaphthalene-1-carbonitrileHCID 684596723-Chloro-4-cyano-2-methylphenylanilineHCID 1317269774-Amino-5,6,7,8-tetrahydronaphthalene-1-carbonitrile, hydrochloride salt

Product 1

HCID 167318492-Chloro-4-isocyanato-3-methylbenzonitrile

Procedure

The title compound was prepared from compound 23D in a manner similar to that described in Experiments 2D to 2E.

Sources & evidence

ORD record
ord-fc08e5365e4a4cf59429d4cad5276564
Source dataset
uspto-grants-2010_08
Patent number
US07772267B2

Reaction notes

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