HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 1-(Benzyloxy)-4-(2-propoxyethoxy)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1-(2-Bromoethoxy)propane | HCID 2734184 | — |
| Reactant | 2-[2-[[2-(2,5-Dihydroxyphenyl)phenyl]methoxymethyl]phenyl]benzene-1,4-diol | HCID 131711022 | — |
| Product | 1-(Benzyloxy)-4-(2-propoxyethoxy)benzene | HCID 19797591 | — |
Reaction Steps
Hydroquinone monobenzyl ether is reacted with 2-bromoethyl-n-propyl ether in aqueous sodium hydroxide and then purified over silica gel with toluene as eluent. The middle fraction gives 1-benzyloxy-4-(2-propoxy-ethoxy)benzene (used without further purification).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05242943 |
| Source dataset | uspto-grants-1993_09 |
| ORD ID | ord-b4b66372e1674802b036ba6406a0f4d5 |
| Source note | uspto-grants-1993_09 |