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1,3-Benzenediamine, N1,N1-dimethyl-, hydrochloride (1:2) → 4-chloro-N-(3-dimethylaminophenyl)-3-(4-propylbenzamido)benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,3-Benzenediamine, N1,N1-dimethyl-, hydrochloride (1:2) | HCID 77124 | — |
| 反応物 | 4-Chloro-3-(4-propylbenzamido)benzoyl chloride | HCID 22636129 | — |
| 生成物 | 4-chloro-N-(3-dimethylaminophenyl)-3-(4-propylbenzamido)benzamide | HCID 9889221 | — |
反応手順
Using an analogous procedure to that described in Example 1, 4-chloro-3-(4-propylbenzamido)benzoyl chloride was reacted with 3-dimethylamino aniline dihydrochloride to give the title compound; NMR Spectrum: DMSOd6) 0.9 (t, 3H), 1.18 (t, 2H), 1.69 (m, 2H), 2.99 (s, 6H), 7.0 (d, 1H), 7.2-7.5 (m, 4H) 7.64-7.8 (m, 3H), 7.84 (d, 1H), 8.0 (m, 2H), 8.19 (s, 1H); Mass Spectrum: M+H+ 436 and 438.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07772432B2 |
| 出典データセット | uspto-grants-2010_08 |
| ORD ID | ord-25f53cf326be430896fd6292580df1a0 |
| 出典メモ | uspto-grants-2010_08 |