2-Naphthoyl chloride → N-(3-dimethylaminophenyl)-4-methyl-3-(2-naphthoylamino)benzamide

HRID 502041Notes

Reaction equation

HRID 502041 reaction equation
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[C:11](Cl)=[O:12].[NH2:14][C:15]1[CH:16]=[C:17]([CH:30]=[CH:31][C:32]=1[CH3:33])[C:18]([NH:20][C:21]1[CH:26]=[CH:25][CH:24]=[C:23]([N:27]([CH3:29])[CH3:28])[CH:22]=1)=[O:19]>>[CH3:29][N:27]([CH3:28])[C:23]1[CH:22]=[C:21]([NH:20][C:18](=[O:19])[C:17]2[CH:30]=[CH:31][C:32]([CH3:33])=[C:15]([NH:14][C:11]([C:2]3[CH:3]=[CH:4][C:5]4[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=4)[CH:1]=3)=[O:12])[CH:16]=2)[CH:26]=[CH:25][CH:24]=1

Participants

3

Reactant 2

HCID 752462-Naphthoyl chlorideHCID 226361113-amino-N-(3-dimethylaminophenyl)-4-methylbenzamide

Product 1

HCID 22636162N-(3-dimethylaminophenyl)-4-methyl-3-(2-naphthoylamino)benzamide

Procedure

Using an analogous procedure to that described in Example 1, 2-naphthoyl chloride was reacted with 3-amino-N-(3-dimethylaminophenyl)-4-methylbenzamide to give the title compound; Mass Spectrum: M+H+ 424.

Sources & evidence

ORD record
ord-5d0f7d069ae249dcb384763801d6e977
Source dataset
uspto-grants-2010_08
Patent number
US07772432B2

Reaction notes

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