HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 18412694, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 18412290 | HCID 18412290 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18412694 | HCID 18412694 | 95% |
Reaction Steps
Prepared analogously to Example 10 from 2-[(4-amidinophenyl)thiomethyl]benzothiazol-5-yl-carboxylic acid-N-phenyl-N-(2-ethoxycarbonylethyl)amide hydrochloride and sodium hydroxide solution. Yield: 95% of theory, C25H22N4O3S2 (490.61); Rf value: 0.25 (Merck RP-8, methanol/5% NaCl solution=6:4); EKA mass spectrum: (M+H)+=491; (M+Na)+=513.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06710055B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-b4df0d18a6734f1688fd0236c77507bf |
| Source note | uspto-grants-2004_03 |