HCID 66613102, compound → HCID 86611054, compound
Reaction equation
CO[CH:3]1[C:12]2C(=CC=C[CH:11]=2)C(C)[CH2:5][CH2:4]1.[CH:14]([C:17]1[CH:31]=[C:30]([CH3:32])[C:29](C=CC=CC)=[CH:28][C:18]=1[O:19][C:20]1[C:21]([NH2:27])=[N:22][C:23]([NH2:26])=[N:24][CH:25]=1)([CH3:16])[CH3:15]>>[CH:14]([C:17]1[CH:31]=[C:30]([CH3:32])[C:29]([C:12]([CH3:11])=[CH:3][CH:4]=[CH2:5])=[CH:28][C:18]=1[O:19][C:20]1[C:21]([NH2:27])=[N:22][C:23]([NH2:26])=[N:24][CH:25]=1)([CH3:16])[CH3:15]Participants
3
Procedure
Similarly prepared, following the procedure of Example 2 but starting with 4-methoxy-1-methyl-1,2,3,4-tetrahydro-naphthalene instead of 7-methoxy-1-methyl-1,2,3,4-tetrahydro-naphthalene, was 5-(2-isopropyl-4-methyl-5-penta-1,3-dienyl-phenoxy)-pyrimidine-2,4-diamine, MP=148° C., MS (M+H)=309.
Workup
- customSimilarly prepared
Sources & evidence
- ORD record
- ord-85098a08f3db409aa94c13c5ff7c1225
- Source dataset
- uspto-grants-2010_08
- Patent number
- US07776872B2
Reaction notes
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