HCID 68458136, compound → HCID 91449898, compound

Participants

Reaction Steps

Prepared by the method of 233 using (1,1-Dioxotetrahydrothiophen-2-yl)methylammonium trifluoroacetate (229). 1H NMR (D2O): 8.28 (1H, s); 7.62 (3H, br s); 7.52-7.40 (4H, m); 6.94 (2H, d, J=10 Hz); 4.42-4.34 (2H, m); 3.84 (1H, dd, J=12, 6 Hz); 3.72 (1H, dd, J=12, 8 Hz); 3.20-3.01 (2H, m); 3.54-3.43 (1H, m); 3.35-3.23 (1H, m); 3.15-3.09 (1H, m); 3.00 (6H, s); 2.48-2.35 (1H, m), 2.30-2.15 (2H, m) and 1.90-1.78 (1H, m). LC/MS: 507 (MH+).

Provenance & Evidence