HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → 1-(2-Thienyl)cyclopent-3-ene-1-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2-Thienylacetonitrile | HCID 72880 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 1-(2-Thienyl)cyclopent-3-ene-1-carbonitrile | HCID 65353080 | — |
Reaction Steps
Thiophene-2-acetonitrile and 1,4-dichloride-2-butene were added to a DMF solution of sodium hydride washed with hexane and the whole was reacted at room temperature to obtain 1-(2-thienyl)cyclopent-3-ene-1-carbonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07776897B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-8008992ec5f640278445eefa7cfdca24 |
| Source note | uspto-grants-2010_08 |