HCID 2795702, compound → 94319-83-2

HRID 502971Notes

Reaction equation

HRID 502971 reaction equation
[Cl:1][C:2]1[CH:20]=[CH:19][CH:18]=[CH:17][C:3]=1[C:4]([NH:6][CH2:7][CH2:8][NH:9]C(=O)OC(C)(C)C)=[O:5].O1CCOCC1.Cl>O1CCOCC1>[ClH:1].[NH2:9][CH2:8][CH2:7][NH:6][C:4](=[O:5])[C:3]1[CH:17]=[CH:18][CH:19]=[CH:20][C:2]=1[Cl:1]

Participants

4

Reactant 2

HCID 2795702HCID 2795702, compoundHCID 204431481,4-Dioxane hydrochloride

Product 1

HCID 1302801194319-83-2

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

tert-Butyl {2-[(2-chlorobenzoyl)amino]ethyl}carbamate was dissolved in dioxane and a 4M hydrogen chloride dioxane solution was added thereto. The whole was stirred at room temperature to obtain N-(2-aminoethyl)-2-chlorobenzamide hydrochloride.

Sources & evidence

ORD record
ord-d5465cd3bef74734b2b4414ceb76ffcd
Source dataset
uspto-grants-2010_08
Patent number
US07776897B2

Reaction notes

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