HuagongsheHuagongshe Chemistry Print Report · For research reference only
[(2-[(6-Bromohexyl)oxy]ethoxy)methyl]benzene → 2-[(6-Bromohexyl)oxy]ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [(2-[(6-Bromohexyl)oxy]ethoxy)methyl]benzene | HCID 46833105 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-[(6-Bromohexyl)oxy]ethanol | HCID 86215509 | 98% |
Reaction Steps
A solution of [(2-[(6-bromohexyl)oxy]ethoxy)methyl]benzene (1.5 g) in EtOAc (20 ml) and EtOH (20 ml) was hydrogenated over 10% palladium on carbon (200 mg). After 2 h the mixture was filtered through celite and the filtrate evaporated in vacuo to give the title compound (1.05 g). TSP+ve 242 (MNH4)+, 244 (MNH4)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07776895B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-358f38fefd1941d9882a49c37a459824 |
| Source note | uspto-grants-2010_08 |