HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol--water (1/1) → 1,17-Biscyclohexylguanidino-9-azaheptadecane triacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol--water (1/1) | HCID 22242641 | — |
| Reactant | 1,17-Biscyclohexylguanidino-9-azaheptadecane dihydroiodide | HCID 131718108 | — |
| Product | 1,17-Biscyclohexylguanidino-9-azaheptadecane triacetate | HCID 131718106 | — |
Reaction Steps
10.2 g (0.011 mol) of 1,17-biscyclohexylguanidino-9-azaheptadecane dihydroiodide in 150 ml of methanol/water (1:1) were filtered through a column containing 250 g of ion exchanger (OH- form). The free guanidine base obtained after working up was dissolved in methanol and converted into the triacetate with excess glacial acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05242948 |
| Source dataset | uspto-grants-1993_09 |
| ORD ID | ord-4bb73f6b08114a6bb1231cd70986f4d3 |
| Source note | uspto-grants-1993_09 |