HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 140409607, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | HCID 18412394 | HCID 18412394 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | HCID 140409607 | HCID 140409607 | 42% |
Reaction Steps
Prepared analogously to Example 90 from 1-methyl-2-[N-(4-amidinophenyl)aminomethyl]benzimidazol-5-yl-carboxylic acid-N-(2-pyridyl)-N-methoxycarbonylmethylamide hydrochloride and ethyl chloroformate. Yield: 42% of theory, C28H29N7O5 (543.6); Rf value: 0.20 (silica gel; dichloromethane/ethanol=19:1); EKA mass spectrum: (M+H)+=544.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06710055B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-bb23f9f9085441e6a13586bb77827163 |
| Source note | uspto-grants-2004_03 |