HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxymandelic acid → n'-[2-Hydroxy-2-(3-hydroxyphenyl)acetyl]-2,4-dibenzyloxy-6-methylbenzohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxymandelic acid | HCID 86957 | — |
| Reactant | 2,4-Dibenzyloxy-6-methylbenzohydrazide | HCID 57461235 | — |
| Product | n'-[2-Hydroxy-2-(3-hydroxyphenyl)acetyl]-2,4-dibenzyloxy-6-methylbenzohydrazide | HCID 57857233 | 47% |
Reaction Steps
The substance is prepared analogously to Example 1 from 2,4-dibenzyloxy-6-methylbenzohydrazide and 3-hydroxymandelic acid in a yield of 47%, m.p. 181-1820 (from Me2COHoEt2O).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07776920B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-140b28ce960345a9ae259a202cc9d626 |
| Source note | uspto-grants-2010_08 |