反应详情

To 14.0 g methyl 3-nitro-1H-pyrazole-5-carboxylate in 200 ml methanol are added 1.2 g Pd/C (10% w/w). The mixture is stirred under H2-atmosphere at room temperature for 18 h. The mixture is filtrated over kieselgur. The filtrate is concentrated and the crude product is used without further purification.

1. filtrationThe mixture is filtrated over kieselgur
2. concentrationThe filtrate is concentrated
3. customthe crude product is used without further purification