Hexyl chloroformate → HCID 140409624, compound

Participants

Reaction Steps

Prepared analogously to Example 90 from 1-methyl-2-[N-(4-amidinophenyl)aminomethyl]benzimidazol-5-yl-carboxylic acid-N-phenyl-N-(3-benzyloxy-n-propyl)amide hydrochloride and n-hexyl chloroformate. Yield: 73% of theory, C40H46N6O4 (674.9); Rf value: 0.46 (silica gel; dichloromethane/ethanol=9:1); EKA mass spectrum: (M+H)+=675; (M+H+Na)++=349; (M+Na)+=697; (M+K)+=713.

Provenance & Evidence