Water → HCID 68466532, compound

HRID 504073Notes

Reaction equation

HRID 504073 reaction equation
O.[CH3:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][C:6]=1[OH:12])=O.O.[NH2:14][CH2:15][C:16]([O-:18])=[O:17].NCC([O-])=O.[Zn+2:24]>C(O)C>[Zn:24].[OH:12][C:6]1[CH:7]=[C:8]([OH:11])[CH:9]=[CH:10][C:5]=1[CH2:3][CH2:2][NH:14][CH2:15][C:16]([OH:18])=[O:17]

Participants

5

Reactant 3

HCID 962WaterHCID 69902',4'-DihydroxyacetophenoneHCID 131728289HCID 131728289, compound

Product 1

HCID 68466532HCID 68466532, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Ingredients. (1) Water 66.18 (2) Ethanol 30.0 (3) Resacetophenone 1.5 (4) Zinc Bis-glycinate Hydrate 2.32. Procedure. The mixture of all ingredients is heated at 80 to 85 C for 2 hours. It is then hydrogenated over Pt catalyst, and after filtration of catalyst N-[(2,4-dihydroxyphenyl)ethyl]glycine zinc complex is obtained.

Workup

  1. additionThe mixture of all ingredients
  2. temperatureis heated at 80 to 85 C for 2 hours
  3. filtrationafter filtration of catalyst N-[(2,4-dihydroxyphenyl)ethyl]glycine zinc complex
  4. customis obtained

Sources & evidence

ORD record
ord-2d4ea1c13e3c4f76bc2e159840c797f3
Source dataset
uspto-grants-2010_08
Patent number
US07777073B2

Reaction notes

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