Beta-Alanine → HCID 86628860, compound

HRID 504084Notes

Reaction equation

HRID 504084 reaction equation
[N+:1]([O-:4])([OH:3])=[O:2].[NH2:5][CH2:6][CH2:7][C:8]([OH:10])=[O:9].[N+:11]([O-:14])([OH:13])=[O:12].[NH2:15][CH2:16][CH2:17][C:18]([OH:20])=[O:19]>O>[N+:1]([O-:4])([OH:3])=[O:2].[N+:11]([O-:14])([OH:13])=[O:12].[NH2:5][CH2:6][CH2:7][C:8]([OH:10])=[O:9].[N+:1]([O-:4])([OH:3])=[O:2].[N+:1]([O-:4])([OH:3])=[O:2].[N+:1]([O-:4])([OH:3])=[O:2].[NH2:15][CH2:16][CH2:17][C:18]([OH:20])=[O:19]

Participants

6

Reactant 3

HCID 239Beta-AlanineHCID 944Nitric AcidHCID 25232619HCID 25232619, compound

Product 2

HCID 86628860HCID 86628860, compoundHCID 86628861HCID 86628861, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Applicants have cost-effectively synthesized Beta Alanine Nitrate by combining nitric acid and Beta Alanine, mixing with water, and leaving to crystallize. Further nitratization can take place, yielding Beta Alanine Dinitrate or Beta Alanine Trinitrate. An alternative implementation comprises using Nitrous Acid (HNO2) instead of Nitric Acid (HNO3), thus yielding Beta Alanine Nitrite. Beta Alanine Nitrite has the same effects as Beta Alanine Nitrate, the only difference being that it requires one less step to yield Nitric Oxide (NO—). Mixed salts may also be used, such as in the non-limiting example of Beta Alanine Nitrate-Orotate.

Workup

  1. customleaving
  2. customto crystallize

Sources & evidence

ORD record
ord-e0772dccbdbf4ab1a2ef5cc7ef10ba68
Source dataset
uspto-grants-2010_08
Patent number
US07777074B2

Reaction notes

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