HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dibromoethane → 1H-Isoindole-1,3(2H)-dione, 2-(2-bromoethoxy)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dibromoethane | HCID 7839 | — |
| Reactant | N-Hydroxyphthalimide | HCID 10665 | — |
| Product | 1H-Isoindole-1,3(2H)-dione, 2-(2-bromoethoxy)- | HCID 199875 | — |
| Product | O-(2-bromoethyl)hydroxylamine hydrobromide | HCID 19077315 | — |
Reaction Steps
2-(2-Bromo-ethoxy)-isoindole-1,3-dione is prepared from 1,2-dibromoethane and N-hydroxyphthalimide as described in WO 00/18790, and is then subjected to the procedure in J. Org. Chem., 1963, 28, 1604 to yield the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07777050B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-247e0e3e743f4362947a523b0670934b |
| Source note | uspto-grants-2010_08 |