HRID504400
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
产物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a solution of methyl 3-[1-(phenoxyacetyl)-2,3-dihydro-1H-pyrrol-3-yl]benzoate (0.5 g, 0.001 mol) in methanol (15 mL, 0.37 mol) was added 10% Pd/C (80 mg), and the resulting suspension was stirred under 1 atm of H2 (balloon) for 5 h. The mixture was filtered and the filtrate was concentrated to afford the desired product.
WORKUP
后处理
- filtrationThe mixture was filtered
- concentrationthe filtrate was concentrated