HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(5-Fluoro-2-methylphenyl)-3-trimethylsilyoxy-2-aza-1,3-butadiene → HCID 86632078, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(5-Fluoro-2-methylphenyl)-3-trimethylsilyoxy-2-aza-1,3-butadiene | HCID 70178504 | — |
| Reactant | HCID 86632077 | HCID 86632077 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86632078 | HCID 86632078 | 1.7% |
Reaction Steps
In a manner similar to the method described in Example 10d, E/Z-6-chloro-3-(5-chloro-2-cyanomethoxy-benzylidene)-2-oxo-2,3-dihydro-indole-1-carboxylic acid tert-butyl ester (5 g, 11 mmol) was reacted with 1-(5-fluoro-2-methyl-phenyl)-3-trimethylsilyoxy-2-aza-1,3-butadiene (44 mmol) in toluene to give the title compound as a white solid (100 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07776875B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-1c2fa5bc5d304bb6a647b7180e15b64b |
| Source note | uspto-grants-2010_08 |