HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 131728300, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 6-Chloro-1,3-dihydroindol-2-one | HCID 736344 | — |
| Reactant | HCID 57750215 | HCID 57750215 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131728300 | HCID 131728300 | 91.3% |
Reaction Steps
In a manner similar to the method described in Example 9b, 5-chloro-2-methanesulfinylmethoxy-benzaldehyde (0.4 g, 1.72 mmol) was reacted with 6-chlorooxindole (0.31 g, 1.86 mmol) and pyrrolidine (0.13 g, 1.86 mmol) in methanol (10 mL) to give the title compound as a yellow solid (0.6 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07776875B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-13988fcfb81c48e68699a63581213e95 |
| Source note | uspto-grants-2010_08 |