HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1',1''-(Chlorosilylidyne)tris(benzene) → 5-Tripenylsilyl-m-xylene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1',1''-(Chlorosilylidyne)tris(benzene) | HCID 6458 | — |
| Reactant | Benzene, 1-bromo-3,5-dimethyl- | HCID 136357 | — |
| Product | 5-Tripenylsilyl-m-xylene | HCID 59171948 | — |
Reaction Steps
In the same manner as described in preparation 1, 5-bromo-m-xylene was allowed to react with chlorotriphenylsilane, and afforded TPSIX. The yield and properties are summarized in Table 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05243010 |
| Source dataset | uspto-grants-1993_09 |
| ORD ID | ord-55b62a5f55db48bfae40873d928c5459 |
| Source note | uspto-grants-1993_09 |