HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 50518Generated: October 27, 2026
Allyl bromide → N-allyl-N-[3-(perfluorooctyl)phenyl]-2,4-dinitrobenzenamine
https://huagongshe.com/reaction/50518
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-[3-(perfluorooctyl)phenyl]-2,4-dinitrobenzenamine | HCID 22735001 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | N-allyl-N-[3-(perfluorooctyl)phenyl]-2,4-dinitrobenzenamine | HCID 22735002 | — |
Reaction Steps
A mixture of N-[3-(perfluorooctyl)phenyl]-2,4-dinitrobenzenamine (5.4 g), allyl bromide (1.5 mL), potassium carbonate (2.6 g) and N-methyl pyrrolidone (15 mL) was heated to 60-70° C. for 5.5 hr. Extraction in the normal fashion gave 5.6 g of N-allyl-N-[3-(perfluorooctyl)phenyl]-2,4-dinitrobenzenamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06713135B2 |
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| Source dataset | uspto-grants-2004_03 |
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| ORD ID | ord-13071fffde304d9fa44f9cbaeeb5f753 |
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| Source note | uspto-grants-2004_03 |
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