Acrolein → HCID 22281041, compound

HRID 50526Notes

Reaction equation

HRID 50526 reaction equation
[CH:1]([O:3][CH:4]1[CH2:9][CH:8]2[CH2:10][CH:5]1[CH:6]=[CH:7]2)=[O:2].[CH:11]([CH:13]=[CH2:14])=[O:12]>>[CH:1]([O:3][CH:4]1[CH:5]2[CH2:10][CH:8]([CH:7]3[CH:6]2[O:12][CH:11]=[CH:13][CH2:14]3)[CH2:9]1)=[O:2]

Participants

3

Reactant 2

HCID 7847AcroleinHCID 548723HCID 548723, compound

Product 1

HCID 22281041HCID 22281041, compoundYield 49%

Procedure

248 g of 5-norbomene-2-yl formate and 33.6 g of acrolein were reacted in the same manner asin Examplel1-1to synthesize adesired product. As aresult, 57 g of 3-oxa-tricyclo[6.2.1.02,7]undec-4-ene-10-yl formate was obtained.

Workup

  1. customsynthesize

Sources & evidence

ORD record
ord-51cf999c4b4c4eb2807f6b59daff936c
Source dataset
uspto-grants-2004_03
Patent number
US06713228B2

Reaction notes

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