Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 178418361, 화합물 → HCID 178453600, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 반응물 | HCID 178453603 | HCID 178453603 | — |
| 촉매 | Platinum oxide (PtO) | HCID 82844 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | HCID 178453600 | HCID 178453600 | — |
반응 단계
trans-(4-Azidomethyl-cyclohexylmethyl)-carbamic acid tert-butyl ester (24 g) in ethyl acetate (1 liter) is hydrogenated over platinumoxide (2.4 g) at ambient temperature under atmospheric pressure of hydrogen. The catalyst is filtered-off and the filtrate concentrated to yield trans-(4-aminomethyl-cyclohexylmethyl)-carbamic acid tert-butyl ester as an oil. Rf(C2) 0.41.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06713265B1 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-50b2e797a8f447b29a716a3d29374ec3 |
| 출처 메모 | uspto-grants-2004_03 |