HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-Ethyl-4-(4-nitrophenyl)-1,2,4-thiadiazolidine-3,5-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | Benzene, 1-isothiocyanato-4-nitro- | HCID 75044 | — |
| Reactant | Potassium Permanganate | HCID 516875 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-Ethyl-4-(4-nitrophenyl)-1,2,4-thiadiazolidine-3,5-dione | HCID 6539173 | — |
Reaction Steps
Reagents: 4-nitrophenyl isothiocyanate (1.17 g, 6.5 mmol), 35% HCl (3.1 ml), KMnO4 (0.5 g), ethyl isocyanate (0.51 ml, 6.5 mmol) in THF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07781463B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-a4e103d00cc74487835c37af8c4f552d |
| Source note | uspto-grants-2010_08 |