HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzyl alcohol → 1-[(4-Methoxyphenyl)methyl]-1H-pyrrole-2,5-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzyl alcohol | HCID 7738 | — |
| Reactant | Maleimide | HCID 10935 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Diethyl azodicarboxylate | HCID 5462977 | — |
| Product | 1-[(4-Methoxyphenyl)methyl]-1H-pyrrole-2,5-dione | HCID 2737837 | — |
Reaction Steps
Reagents: Ph3P (1.31 g, 5 mmol), DEAD (0.8 ml, 5 mmol), p-methoxybenzyl alcohol (0.93 ml, 7.5 mmol) and maleimide (0.48 g, 5 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07781463B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-c6bee78d157a4729b974342c8a1b900e |
| Source note | uspto-grants-2010_08 |