HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-Formylbenzoate → Methyl 4-({[2-(5-fluoro-2-methoxyphenyl)ethyl]imino}methyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-Formylbenzoate | HCID 15294 | — |
| Reactant | 2-(5-Fluoro-2-methoxyphenyl)ethan-1-amine | HCID 22015010 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Methyl 4-({[2-(5-fluoro-2-methoxyphenyl)ethyl]imino}methyl)benzoate | HCID 22014991 | — |
Reaction Steps
9.00 g (53 mmol) of 2-(5-fluoro-2-methoxyphenyl)ethylamine and 8.73 g (53 mmol) of methyl 4-formylbenzoate are dissolved in 450 ml of ethanol, the mixture is heated at reflux for 2 hours and the solvents are then evaporated under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07781470B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-e524e8956d144e79be95e7b0fb3a58d2 |
| Source note | uspto-grants-2010_08 |